Types of Analysis Methods

Main Analysis Methods

  • SPME-GC/MSMS with a sniffing system
  • Solvent extraction-GCMS
  • SPME-Olfactory GCMS
  • Distillation-GCMS

About SPME-GCMS Method

Solid-Phase microextraction (SPME, SPME-Arrow) is available as a method for identifying odor components.
Solid-phase microextraction enables analysis of ultra-trace components by adsorbing and concentrating volatile components (odor substances).

GCMS instrument for analysis. CMS(with a sniffing system)

The GC column outlet is split into two branches and ventilated to a sniffing port. By comparing MS data with human sensory perception, it becomes possible to identify off-odor causative substances with higher precision.


Flow diagram of GCMS equipment (GCSMS) 
Flow diagram of GCMS equipment (GCSMS) SPME-GCMS with a sniffing system

The GCMS results diagram is called a “gas chromatogram” (shown below).
Each peak substance is identified and conclusions are drawn in combination with sensory testing results.

In this case, we detected “benzyl alcohol,” “dihydromyrcenol,” and “linalool” from damaged coffee beans, which are not contained in normal products. All of these substances have floral fragrances. Since these are substances contained in fragrances, contamination from fragrances themselves or fabric softeners and cosmetic products containing them is suspected.

Graph showing the detection of [dihydroxyacetone,] 「benzaldehyde,」 and [ribulose] from coffee beans Graph showing the detection of [dihydroxyacetone,] 「benzaldehyde,」 and [ribulose] from coffee beans Sample 1: Coffee Beans (Damaged Goods)
Graph of authentic coffee beans Graph of authentic coffee beans Sample 2: Coffee Beans (Sound Goods)
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